The Friščić group publications
2025
2025
J. M. Marrett, F. Effaty, X. Ottenwaelder*, T. Friščić* “Mechanochemistry for Metal–Organic Frameworks and Covalent–Organic Frameworks (MOFs, COFs): Methods, Materials, and Mechanisms” Adv. Mater., 2025, 2418707, DOI: 10.1002/adma.202418707
I. Brekalo*, K. Lisac, J. R. Ramirez, P. Pongrac, A. Puškarić. S. Valić, Y. Xu, M. Ferguson, J. M. Marrett, M. Arhangelskis*, T. Friščić*, and K. T. Holman “Mechanochemical Solid Form Screening of Zeolitic Imidazolate Frameworks Using Structure-Directing Liquid Additives” J. Am. Chem. Soc., 2025, 147, 27413–27430, DOI: 10.1021/jacs.5c04043
T. H. Borchers*, F. Topić, M. Arhangelskis, M. Ferguson, C. B. Lennox, P. A. Julien, and T. Friščić* “Terahertz-Raman spectroscopy for in situ benchtop monitoring of changes to extended, supramolecular structure in milling mechanochemistry” Chem. 2025, 11, 102319, DOI: 10.1016/j.chempr.2024.09.018
T. Manyepedza, T. Auvray, r. Hendim G. N. Aliev, T. Friščić, and N. V. Rees* “Novel electrocatalysts via mechanochemistry: Binary & ternary mixed transition metal dichalcogenides” Appl. Mater. Today. 2025, 42, 102582, DOI: 10.1016/j.apmt.2025.102582
K. R. Floyd, L. S. Mella, R. W. Kwok, M. Gray, E. J. Broker Jr. , M. Marianski, T. Friščić, and J. D. Batteas* “Harnessing the copper surface for direct mechanocatalysis: a case study on mechanochemical sulfonylurea synthesis” Chem. Sci., 2025, DOI: 10.1039/D5SC04099J
M. H. Gohari, P. Ghamari, E. Hamzehpoor, F. Effaty, T. Friščić, and D. F. Perepichka “Mechanochemical synthesis of π-conjugated naphthotetrathiophene-based covalent organic frameworks and their post-modification via the Doebner reaction” Chem. Sci., 2025, 16, 18101-18112, DOI: 10.1039/D5SC04390E
A. A. L. Michalchuk, and T. Friščić “Moving Mechanochemistry Forward: Mechanochemistry and the non-covalent bond” RSC Mechanochem., 2025,2, 333-335 DOI: 10.1039/D5MR90011E
J. Batteas, and T. Friščić “Shaken not stirred: procedures in mechanochemical syntheses and how to define them” RSC Mechanochem., 2025, 2, 175-177, DOI: 10.1039/D5MR90005K
J. Batteas, K. G. Blank, E. Colacino, F. Emmerling, T. Friščić, J. Mack, J. Moore, M. E. Rivas, and W. Tysoe “Moving mechanochemistry forward” RSC Mechanochem., 2025, 2, 10-19, DOI: 10.1039/D4MR90021A
2024
2024
D. Farajat, J-L. Do, P. Forgione, T. Friščić*, L. A. Cuccia*, and C-J. Li.* “Shaking Up the Friedländer Reaction: Rapid, Scalable Mechanochemical Synthesis of Polyaryl-Substituted Quinolines” Adv. Synth. Catal., 2024, 366, 5135-5143, DOI: 10.1002/adsc.202400862
E. Hamzehpoor, F. Effaty, T. H. Borchers, R. S. Stein, A. Wahrhaftig-Lewis, X. Ottenwaelder*, T. Friščić*, and D. F. Perepichka* “Mechanochemical Synthesis of Boroxine-linked Covalent Organic Frameworks” Angew. Chem. Int. Ed., 63, e202404539, DOI: 10.1002/anie.202404539
J. Vainauskas, A. Wahrhaftig-Lewis, and T. Friščić* “Utilizing “Latent” Carbon: Repositioning Hydrogen-Bonded Synthons and Assemblies via Halogen Bonding to π-Systems” Angew. Chem. Int. Ed., 63, e202408053, DOI: 10.1002/anie.202408053
T. Manyepedza, T. Auvray, T. Friščić, N. V. Rees* “Electrochemically deposited transition metal dichalcogenide heterostructures as electrocatalysts: Accelerated kinetics for the hydrogen evolution reaction” Electochem. Commun., 2024, 160, 107678, DOI: 10.1016/j.elecom.2024.107678
O. Al Rahal, M. Ferguson, C. B. Lennox, L. Male, T. Friščić * “Structure of the caffeine–pyrogallol complex: revisiting a pioneering structural analysis of a model pharmaceutical cocrystal” Chem. Commun., 2024, 60, 7431-7434, DOI: 10.1039/D4CC02289K
K. Floyd, L. Gonnet, T. Friščić*, and J. Batteas* “The role of the milling environment on the copper-catalysed mechanochemical synthesis of tolbutamide” RSC Mechanochem., 2024, 1, 289-295, DOI: 10.1039/D4MR00031E
D. Szczerba, J-L. Do, D. Tan, H. M. Titi, N. Geoffroy, M. C. M. de Lucas, J. Boudon, I Halasz, T. Friščić*, S. A. J. Kimber* “Mechanochemical synthesis of bismuth active pharmaceutical ingredients, bismuth(III) gallate and bismuth citrate” RSC Mechanochem., 2024, 1, 255-262, DOI: 10.1039/D4MR00008K
J. Batteas*, and T. Friščić* “Introducing RSC Mechanochemistry”, RSC Mechanochem., 2024, 1, 9-10, DOI: 10.1039/D4MR90001D
S. Sobczak, A. M. Fidelli, J-L. Do, G. P. Demopoulos*, A. Moores*, T. Friščić*, A. Katrusiak* “High-pressure observation of elusive iodoplumbic acid in different hydronium-hydrate solid forms” Inorg. Chem. Front., 2024, 11, 735-744, DOI: 10.1039/D3QI01102J
J. M. Marrett, H. M. Titi, Y. Teoh, T. Friščić “Supramolecular “baking powder”: a hexameric halogen-bonded phosphonium salt cage encapsulates and functionalises small-molecule carbonyl compounds” Chem. Sci., 2024, 15, 298-306, DOI: 10.1039/D2SC04615F
M. Ferguson*, and T. Friščić* ”Exploring mechanochemistry of pharmaceutical cocrystals: effect of incident angle on molecular mixing during simulated indentations of two organic solids” Phys. Chem. Chem. Phys., 2024, 26, 9940-9947, DOI: 10.1039/D3CP05475F
M. E. Leger, J. Guo, B. MacMillan, H. M. Titi, T. Friščić, B. Balcom,* and B.A. Blight.* “In situ monitoring of mechanochemical MOF formation by NMR relaxation time correlation” Phys. Chem. Chem. Phys., 2024, 26, 543-550, DOI: 10.1039/D3CP05555H
2023
2023
M. A. Sadeghi, Z. A.Khan, M. Agnaou, L. Hu, S. Litster, A. Kongkanand, E. Padgett, D. A. Muller, T. Friščić, and J. Gostick* "Predicting PEMFC performance from a volumetric image of catalyst layer structure using pore network modeling" Appl. Energy 2024, 353, doi:10.1016/j.apenergy.2023.122004
J. M. Marrett, H. M. Titi, Y. Teoh, and T. Friščić* “Supramolecular “baking powder”: a hexameric halogen-bonded phosphonium salt cage encapsulates and functionalises small-molecule carbonyl compounds” Chem. Sci., 2024,15, 298-306, DOI: 10.1039/D2SC04615F
T. H. Borchers, F. Topic, M. Arhanfelskis, J. Vainauskas, H. M. Titi, O. S. Bushuyev, C. J. Barrett*, and T. Friščić* “Three-in-One: Dye-Volatile Cocrystals Exhibiting Intensity-Dependent Photochromic, Photomechanical, and Photocarving Response” J. Am. Chem. Soc. 2023, 145, 24636–24647 DOI: 10.1021/jacs.3c07060
J. Vainauskas, T. H. Borchers, M. Arhanfelskis, L. J. McCormick McPherson, T. S. Spilfogel, E. Hamzehpoor, F. Topić, S. J. Coles, D. F. Perepichka, C. J. Barrett, and T. Friščić* “Halogen bonding with carbon: directional assembly of non-derivatised aromatic carbon systems into robust supramolecular ladder architectures” Chem. Sci., 2023,14, 13031-13041, DOI: 10.1039/D3SC04191C
P. A. Julien*, M. Arhangelskis*, L. S. Germann, M. Etter, R. E. Dinnebier, A. J. Morris, and T. Friščić* “Illuminating milling mechanochemistry by tandem real-time fluorescence emission and Raman spectroscopy monitoring” Chem. Sci., 2023, 14, 12121-12132, DOI: 10.1039/D3SC04082H
G. J. Leonel, C. B. Lennox, Y. Xu, M. Arhangelskis*, T. Friščić*, and A. Navrotsky* “Experimental and Theoretical Evaluation of the Thermodynamics of the Carbonation Reaction of ZIF-8 and Its Close-Packed Polymorph with Carbon Dioxide” J. Phys. Chem. C., 2023, 127, 19520–19526, DOI: 10.1021/acs.jpcc.3c04135
G. J. Leonel, C. B. Lennox, M. Scharrer, K. Jayanthi, T. Friščic*, and A. Navrotsky* "Experimental Investigation of Thermodynamic Stabilization in Boron Imidazolate Frameworks (BIFs) Synthesized by Mechanochemistry" J. Phys. Chem. C. 2023, 127, doi:10.1021/acs.jpcc.3c04164
G. J. Leonel, C. B. Lennox, J. M. Marrett, T. Friščić*, A. Navrotsky* "Crystallographic and Compositional Dependence of Thermodynamic Stability of [Co(II), Cu(II), and Zn(II)] in 2-Methylimidazole-Containing Zeolitic Imidazolate Frameworks" Chem. Mater. 2023, 35, doi:10.1021/acs.chemmater.3c01464
R. A. Hernandez, I. Trakakis, J.-L. Do, L. Cuccia, T. Friščić, P. Forgione* "Mechanochemical Desymmetrization of Unbiased Bis- and Tris-alkynes to Access 3,5-Isoxazoles-Alkyne Adducts and Unsymmetrical Bis-3,5-isoxazoles" Eur. J. Org. Chem. 2023, 26, doi:10.1002/ejoc.202300374
M. Pérez-Venegas, T. Friščić*, K. Auclair* "Efficient Mechano-Enzymatic Hydrolysis of Polylactic Acid under Moist-Solid Conditions" ACS Sustainable Chem. Eng. 2023, 11, doi:10.1021/acssuschemeng.2c06847
Y. Xu, J. M. Marrett, H. M. Titi, J. P. Darby, A. J. Morris*, T. Friščić*, M. Arhangelskis* "Experimentally Validated Ab Initio Crystal Structure Prediction of Novel Metal–Organic Framework Materials" J. Am. Chem. Soc. 2023, 145, doi:10.1021/jacs.2c12095
T. Auvray, T. Friščić* "Shaking Things from the Ground-Up: A Systematic Overview of the Mechanochemistry of Hard and High-Melting Inorganic Materials" Mol. 2023, 28, doi:10.3390/molecules28020897
C. B. Lennox, T. H. Borchers, L. Gonnet, C. J. Barrett, S. G. Koenig, K. Nagapudi*, T. Friščić* "Direct mechanocatalysis by resonant acoustic mixing (RAM)" Chem. Sci. 2023, 14, doi:10.1039/D3SC01591B
J. -L. Do, T. Auvray, C. B. Lennox, H. M. Titi, L. A. Cuccio, T. Friščić* "Rapid, room-temperature, solvent-free mechanochemical oxidation of elemental gold into organosoluble gold salts" Green Chem. 2023, 25, doi:10.1039/D3GC01150J
A. J. Richard, M. Ferguson, B. G. Fiss, H. M. Titi, J. Valdez, N. Provatas, T. Friščić*, A. Moores* "In situ study of Au nanoparticle formation in a mechanochemical-aging-based method" Nanoscale Adv. 2023, 5, doi:10.1039/D2NA00759B
S. Kaabel, J. Arciszewski, T. H. Borchers, J. P. D. Therien, T. Friščić*, K. Auclair* "Solid-State Enzymatic Hydrolysis of Mixed PET/Cotton Textiles" ChemSusChem 2022, 1, doi:10.1002/cssc.202201613
2022
2022
F. Effaty, L. Gonnet, S. G. Koenig, K. Nagapudi, X. Ottenwaelder*, T. Friščić* "Resonant acoustic mixing (RAM) for efficient mechanoredox catalysis without grinding or impact media" Chem. Comm. 2022, 8, doi:10.1039/D2CC06013B
S. Kaabel, J. Arciszewski, T. H. Borchers, J. P. D. Therien, T. Friščić*, K. Auclair* "Solid-State Enzymatic Hydrolysis of Mixed PET/Cotton Textiles" ChemSusChem 2022, 16, e202201613. doi:10.1002/cssc.202201613
S. Muratović, V. Martinez, B. Karadeniz, D. Pajić, I. Brekalo, M. Arhangelskis, M. Mazaj, G. Mali, M. Etter, T. Friščić, Y. Krupskaya, V. Kataev, D. Žilić*, K. Užarević* "Low-Dimensional Magnetism in Multivariate Copper/Zinc MOF-74 Materials Formed via Different Mechanochemical Methods" Inorg. Chem. 2022, 61, 18181–18192. doi:10.1021/acs.inorgchem.2c028985
B. G. Fiss, G. Douglas, M. Ferguson, J. Becerra, J. Valdez, T.-O. Do*, T. Friščić*, A. Moores* "Mechanosynthesis of a Structurally Characterized, Well-Defined Graphitic Phosphorus-Linked Carbon Nitride (g-PCN) with Water Splitting Activity" Adv. Mater. Interfaces 2022, 9, 2201555. doi:10.1002/admi.202201555
J. Vainauskas, F. Topić, M. Arhangelskis, H. M. Titi, T. Friščić* "Polymorphs and solid solutions: materials with new luminescent properties obtained through mechanochemical transformation of dicyanoaurate(i) salts" Faraday Discuss. 2022, 241, 425-447. doi:10.1039/D2FD00134A
B. G. Fiss, G. Douglas, M. Ferguson, J. Becerra, J. Valdez, T.-O. Do*, T. Friščić*, A. Moores* "Mechanochemical bottom-up synthesis of phosphorus-linked, heptazine-based carbon nitrides using sodium phosphide" Beilstein J. Org. Chem. 2022, 18, 1203-1209. doi:10.3762/bjoc.18.125
G. S. Lee, H. W. Lee, T. Do, J.-L. Do, J. Lim, G. I. Peterson, T. Friščić*, J. G. Kim* "Mechanochemical ring-opening metathesis polymerization: development, scope, and mechano-exclusive polymer synthesis" Chem. Sci. 2022, 13, 11496-11505. doi:10.1039/D2SC02536A
P. A. Julien*, T. Friščić* "Methods for Monitoring Milling Reactions and Mechanistic Studies of Mechanochemistry: A Primer" Cryst. Growth Des. 2022, 9, 5726-5754. doi:10.1021/acs.cgd.2c00587
Y. Teoh, G. Ayoub, I. Huskić, H. M. Titi, C. W. Nickels, B. Herrmann, T. Friščić* "SpeedMixing: Rapid Tribochemical Synthesis and Discovery of Pharmaceutical Cocrystals without Milling or Grinding Media" Angew. Chem., Int. Ed. 2022, 61, e202206293. doi:10.1002/anie.202206293
T. H. Borchers, F. Topic, J.-C. Christopherson, O. S. Bushuyev, J. Vainauskas, H. M. Titi, T. Friščić*, C. J. Barrett* "Cold photo-carving of halogen-bonded co-crystals of a dye and a volatile co-former using visible light" Nat. Chem. 2022, 14, 574-581. doi:10.1038/s41557-022-00909-0
S. Lukin, L. S. Germann, T. Friščić*, I. Halasz* "Toward Mechanistic Understanding of Mechanochemical Reactions Using Real-Time In Situ Monitoring" Acc. Chem. Res. 2022, 55, 1262-1277. doi:10.1021/acs.accounts.2c00062
O. Jobin, C. Mottillo, H. M. Titi, J. M. Marrett, M. Arhangelskis, R. D. Rogers*, B. Elzin, T. Friščić*, E. Robert* "Metal–organic frameworks as hypergolic additives for hybrid rockets" Chem. Sci. 2022, 13, 3424-3436. doi:10.1039/D1SC05975K
L. Gonnet, C. B. Lennox, J.-L. Do, I. Malvestiti, S. G. Koenig, K. Nagapudi, T. Friščić* "Metal-Catalyzed Organic Reactions by Resonant Acoustic Mixing" Angew. Chem., Int. Ed. 2022, 61, e202115030. doi:10.1002/anie.202115030
M. Ferguson, A. J. Richard, J. Valdez, B. G. Fiss, H. M. Titi, N. Provatas, T. Friščić*, A. Moores* "Direct observation by high resolution transmission electron microscopy of gold(iii) particle transformation during aging reduction reaction" Faraday Discuss. 2022, 241, 278-288. doi:10.1039/D2FD00126H
2021
2021
D. Szczerba, D. Tan , J.-L. Do, H. M. Titi, S. Mouhtadi, D. Chaumont, M. C. Marco De Lucas, N. Geoffroy, M. Meyer, Y. Rousselin, J. M. Hudspeth, V. Schwanen, P. Spoerk-Erdely, A.-C. Dippel, O. Ivashko, O. Gutowski, P. Glaevecke, V. Bazhenov, M. Arhangelskis, I. Halasz, T. Friščić*, S. A. J. Kimber* "Real-Time Observation of “Soft” Magic-Size Clusters during Hydrolysis of the Model Metallodrug Bismuth Disalicylate" J. Am. Chem. Soc. 2021, 143, 16332–16336. doi:10.1021/jacs.1c07186
C. B. Lennox, J.-L. Do, J. G. Crew, M. Arhangelskis, H. M. Titi, A. J. Howarth O. K. Farha, T. Friščić* "Simplifying and expanding the scope of boron imidazolate framework (BIF) synthesis using mechanochemistry" Chem. Sci. 2021, 12, 14499-14506. doi:10.1039/D1SC03665C
F. Topic, J. M. Marrett, T. H. Borchers, H. M. Titi, C. J. Barrett, T. Friščić* "After 200 Years: The Structure of Bleach and Characterization of Hypohalite Ions by Single‐Crystal X‐Ray Diffraction" Angew. Chem., Int. Ed. 2021, 60, 24400-24405. doi:10.1002/anie.202108843
F. Effaty, X. Ottenwaelder*, T. Friščić* "Mechanochemistry in transition metal catalyzed reactions" Curr. Opin. Green Sust.. 2021, 32, 100524. doi:10.1016/j.cogsc.2021.100524
B. G. Fiss, A. J. Richard, G. Douglas, M. Kojic, T. Friščić*, A. Moores* "Mechanochemical methods for the transfer of electrons and exchange of ions: inorganic reactivity from nanoparticles to organometallics" Chem. Soc. Rev. 2021, 50, 8279-8318. doi:10.1039/D0CS00918K
S. Kaabel, J. P. D. Therien, C. E. Deschênes, D. Duncan, T. Friščić*, K. Auclair* "Enzymatic depolymerization of highly crystalline polyethylene terephthalate enabled in moist-solid reaction mixtures" Proc. Natl. Acad. Sci. U. S. A. 2021, 118. doi:10.1073/pnas.2026452118
J.-L. Do, H. M. Titi, L. A. Cuccia*, T. Friščić* "A new class of anionic metallohelicates based on salicylic and terephthalic acid units, accessible in solution and by mechanochemistry" Chem. Commun. 2021, 57 5132-5146. doi:10.1039/D0CC08180A
S. T. Emmerling, L. S. Germann, P. A. Julien, I. Moudrakovski, M. Etter, T. Friščić, R. E. Dinnebier, B. V. Lotsch* "In Situ Monitoring of Mechanochemical Covalent-Organic Framework Formation Reveals Profound Templating Effect of Liquid Additive" Chem 2021, 7 1639-1652. doi:10.1016/j.chempr.2021.04.012
L. Yang*, A. Moores, T. Friščić, N. Provatas* "Thermodynamics Model for Mechanochemical Synthesis of Gold Nanoparticles: Implications for Nanoparticle Production" ACS Appl. Nano Mat. 2021, 4, 1886-1897. doi:10.1021/acsanm.0c03255
T. S. Spilfogel, H. M. Titi*, T. Friščić* "Database Investigation of Halogen Bonding and Halogen···Halogen Interactions between Porphyrins: Emergence of Robust Supramolecular Motifs and Frameworks" Cryst. Growth Des. 2021, 21, 1810-1832. doi:10.1021/acs.cgd.0c01697
C. L. Mertzenich, G. S. Papaefstathiou, T. Friščić, T. D. Hamilton, D.-K. Bučar, D. C. Swenson, L. R. MacGillivray* "Inverted Metal-Organic Frameworks: Isoreticular Decoration with Organic Anions using Principles of Supramolecular Chemistry" J. Coord. Chem. 2021, 74, 169-177. (invited) doi:10.1080/00958972.2021.1880004
T. Stolar, A. Prašnikar, V. Martinez, B. Karadeniz, A. Bjelić, G. Mali, T. Friščić, B. Likozar*, K. Užarević* "Mechanochemical amorphization of bimetallic MOF-74 catalyst for enhanced and selective hydrogenation of CO2 to methanol" ACS Adv. Mat. Int. 2021, 13, 3070-3077. doi:10.1021/acsami.0c21265
T. Xie, S. E. Nikitin, A. I. Kolesnikov, E. Mamontov, L. M. Anovitz, G. Ehlers, I. Huskić, T. Friščić, A. Podlesnyak* "Direct determination of the zero-field splitting for Fe3+ ion in a synthetic polymorph of the oxalate mineral stepanovite NaMgFe(C2O4)3·9H2O: a natural MOF" Phys. Rev. B 2021, 103, 024402. doi:10.1103/PhysRevB.103.024402
B. G. Fiss, A. Richard, T. Friščić*, A. Moores* "Mechanochemistry for sustainable, efficient dehydrogenation/hydrogenation" Can. J. Chem 2021, 99, 93-112. (invited) doi:10.1139/cjc-2020-0408
L. Catalano, L. S. Germann, P. A. Julien, M. Arhangelskis, I. Halasz, K. Užarević, M. Etter, R. E. Dinnebier, M. Ursini, M. Cametti, J. Martí-Rujas, T. Friščić*, P. Metrangolo*, G. Resnati, G. Terraneo* "Open vs. Interpenetrated: Switchable Supramolecular Trajectories in Mechanosynthesis of a Halogen-Bonded Borromean Rings Network" Chem 2021, 7, 146-154. doi:10.1016/j.chempr.2020.10.022
Book Chapters
Book Chapters
I. Halasz, S. Lukin, T. Friščić “In Situ Monitoring of Mechanochemical Ball-Milling Reactions” in: Mechanochemistry and Emerging Technologies for Sustainable Chemical Manufacturing, Editor: E. Colacino, F. Garcia, CRC Press (2023), 3-40
T. Friščić* “Mechanochemistry in cocrystal synthesis” in: Co-crystals – Preparation, Characterization and Applications: Monographs in Supramolecular Chemistry, Editor: C. B. Aakeröy, A. S. Sinha, RSC (2018), 147-193
D. Tan, T. Friščić* “Mechanochemically-enhanced organic transformations” in: Sustainable Catalysis: Energy efficient reactions and Applications, Editors: F. Lam and R. Luque, John Wiley & Sons, New York (2018), 155-176
C. Mottillo, T. Friščić* “Supramolecular Mechanochemistry” in: Comprehensive Supramolecular Chemistry II, Editor: L. Barbour, Elsevier (2017), 101-137
I. Huskić, T. Friščić* “Carbon: Inorganic Chemistry” in: The Encyclopedia of Inorganic and Bioinorganic Chemistry, Editor: R. A. Scott, John Wiley & Sons, New York (2015)
T. Friščić, P. Julien, C. Mottillo “Environmentally-friendly designs and syntheses of metal-organic frameworks (MOFs)", in: Green Technologies for the Environment, Eds.: R. Luque & S. O. Obare, ACS Symposium Series (2014)
T. Friščić “Ball milling mechanochemical synthesis of coordination bonds: discrete units, polymers and porous materials", in: Ball Milling Towards Green Synthesis, Eds.: A. Stolle & B. Ranu, RSC Publishing (2014)
T. Friščić “Mechanochemical approaches to metal-organic frameworks", in: Metal-organic framework materia ls Eds.: C. Lukehart & L. R. MacGillivray and Encyclopedia of Inorganic and Bioinorganic Chemistry, Ed. R. A. Scott, John Wiley & Sons (2014)
T. Friščić “Chemistry through ball milling", McGraw-Hill Yearbook of Science & Technology", McGraw-Hill (2013)
T. Friščić, D. B. Varshney, E. Elacqua, J. C. Sumrak, A. N. Sokolov, L. R. MacGillivray “Molecular Self-Assemblies in Co-Crystals: Engineering Chemical Reactivity and Organic Semiconductor Materials”, in: "Molecular Self-Assembly: Advances and Application" Ed. Alex Li, Pan Stanford Publishing (2012)
D. B. Varshney, J. R. G. Sander, T. Friščić, L. R. MacGillivray “Supramolecular Interactions”, in: "Supramolecular Chemistry: From Molecules to Nanomaterials" Eds. Jonathan W. Steed & Philip Gale, Wiley (2012)
T. Friščić, W. Jones “Development of liquid-assisted grinding (LAG) for the synthesis of hydrogen-bonded and coordination frameworks", in: "Frontiers in Mechanochemistry and Mechanical Alloying", published by International Mechanochemistry Association and National Metallurgy Laboratory, India (2011)
T. Friščić, W. Jones “Application of mechanochemistry in the synthesis and discovery of new pharmaceutical forms: cocrystals, salts and coordination compounds”, in: "Pharmaceutical salts and cocrystals" Eds. Johan Wouters & Luc Quere, RSC (2011).
(B) L. Fábián, T. Friščić “Shape and Polarity in Cocrystal Formation: Database Analysis and Experimental Validation”, in: "Pharmaceutical salts and cocrystals" Eds. Johan Wouters & Luc Quere, RSC (2011)
T. Friščić “Towards mechanochemical synthesis of metal-organic frameworks (MOFs): from coordination polymers and lattice inclusion compounds to porous materials”, in: "Metal-Organic Frameworks: Design and Application" Ed. Leonard R. MacGillivray, John Wiley & Sons (2010)
T. Friščić, L. R. MacGillivray* "Supramolecular approaches to building crystalline solids from crystalline solids" in: "Making crystals by design – from molecules to molecular materials, methods, techniques, applications", Eds. D. Braga and F. Grepioni, Wiley-VCH, Weinheim (2007).
T. Friščić, L. R. MacGillivray* “Template-Controlled Solid-State Synthesis: Towards a General Form of Covalent Capture in Molecular Solids” in: Frontiers in Crystal Engineering, E. R. T. Tiekink and J. J. Vittal, Eds., John Wiley & Sons, New York (2006)
T. Friščić, L. R. MacGillivray* “The Inorganic Chemistry of Carbon” in: The Encyclopedia of Inorganic Chemistry, 2nd Edition, Editor: R. B. King, John Wiley & Sons, New York (2005)
Archive
Archive
2020
N. Novendra, J. M. Marrett, A. D. Katsenis, H. M. Titi, M. Arhangelskis, T. Friščić*, A. Navrotsky* "Linker Substituents Control Thermodynamic Stability in Metal-Organic Frameworks" J. Am. Chem. Soc. 2020, 142, 21720-21729. doi:10.1021/jacs.0c09284
O. Abate Fulas, A. Laferriere, G. Ayoub, G. Dayaker, C. Mottillo, H. M. Titi, R. S. Stein, T. Friščić*, T. J. Coderre* "Drug- nutraceutical co-crystal and salts for making new and improved bi-functional analgesics" Pharmaceutics 2020, 12, 1144. (invited) doi:10.3390/pharmaceutics12121144
J. Vainauskas, F. Topić, O. S. Bushuyev, C. J. Barrett*, T. Friščić* "Halogen bonding to the azulene π-system: cocrystal design of pleochroism" Chem. Commun. 2020, 56, 15145-15148. doi:10.1039/D0CC04758A
I. Huskić, C. B. Lennox, T. Friščić* "Accelerated ageing reactions: towards simpler, solvent- and energy-free chemistry" Green Chem. 2020, 22, 5881-5901. doi:10.1039/D0GC02264K
L. S. Germann*, M. Arhangelskis, R. S. Stein, M. Etter, R. E. Dinnebier, T. Friščić* “Challenging the Ostwald rule of stages in mechanochemical cocrystallisation“ Chem. Sci. 2020, 11, 10092-10100. doi:10.1039/D0SC03629C (cover page)
S. Lukin, T. Stolar, I. Lončarić, I. Milanović, N. Biliškov, M. di Michiel, T. Friščić, I. Halasz* “Mechanochemical metathesis between AgNO3 and NaX (X = Cl, Br, or I), and Ag2XNO3 double salt formation“ Inorg. Chem. 2020, 59, 12200-12208. doi: 10.1021/acs.inorgchem.0c01196
B. G. Fiss, N. N. Vu, G. Douglas, T.-O. Do, T. Friščić*, A. Moores* “Solvent-free mechanochemical synthesis of ultrasmall nickel phosphide nanoparticles and their application as a catalyst for the hydrogen evolution reaction (HER)“ ACS Sust. Chem. Eng. 2020, 8, 12014-12024
M. Arhangelskis, F. Topić, P. Hindle, R. Tran, A. J. Morris, D. Cinčić*, Tomislav Friščić* “Understanding reactions of cocrystals: comparing theory with experiment in the making and breaking halogen bonds in the solid state“ Chem. Commun. 2020, 56, 8293-8296. doi:10.1039/D0CC02935A
J. P. Darby, M. Arhangelskis, A. D. Katsenis, J. M. Marrett, T. Friščić, A. J. Morris* “Ab initio prediction of metal-organic framework structures“ Chem. Mater. 2020, 32, 5835-5844. doi:10.1021/acs.chemmater.0c01737
F. Hammerer, S. Ostadjoo, K. Dietrich, M.-J. Dumont, L. F. Del Rio, T. Friščić*, K. Auclair* “Rapid mechano-enzymatic saccharification of lignocellulosic biomass without bulk water or chemical pre-treatment“ Green Chem. 2020, 22, 3877-3884. doi:10.1039/D0GC00903B
I. Huskić, M. Arhangelskis, T. Friščić* “Solvent-free ageing reactions of rare earth element oxides: From geomimetic synthesis of new metal-organic materials towards a simple, environmentally-friendly separation of scandium“ Green Chem. 2020, 22, 4364-4375. doi:10.1039/D0GC00454E
V. Nemec, T. Piteša, T. Friščić, D. Cinčić* “The morpholinyl oxygen atom as an acceptor site for halogen-bonded cocrystallization of organic and metal–organic Units“ Cryst. Growth Des. 2020, 20, 3617-3624. doi:10.1021/acs.cgd.0c00520
D. Gandrath, D. Tan, N. Biggins, A. Shelam, J.-L. Do, A. D. Katsenis, T. Friščić* ”Catalytic room‐temperature C‐N coupling of amides and isocyanates using mechanochemistry" ChemSusChem 2020, 13, 2966-2972. doi:10.1002/cssc.201902576
A. J. Cruz-Cabeza*, M. D. Ward*, A. Lemmerer*, T. Friščić* "A Truly Polymorphic Issue in Honor of Prof Joel Bernstein" Cryst. Growth Des. 2020, 20, 2819–2823, doi:10.1021/acs.cgd.0c00340
C. A. O’Keefe, C. Mottillo, L. Fábián, T. Friščić*, R. W. Schurko* “NMR-Enhanced Crystallography Aids Open Metal-Organic Framework Discovery Using Solvent-Free Accelerated Aging“ Chem. Mater. 2020, 32, 4273–4281 doi:10.1021/acs.chemmater.0c00894
J. D. Thorpe, D. O'Reilly, T. Friščić*, M. J. Damha* “Mechanochemical synthesis of short DNA fragments“ Chem. Eur. J. 2020, 26, 8857-8861. doi:10.1002/chem.202001193
P. F. Rosen, M. S. Dickson, J. J. Calvin, N. L. Ross, T. Friščić, A. Navrotsky, B. F. Woodfield* “Thermodynamic Evidence of Structural Transformations in CO2-Loaded Metal–Organic Framework Zn(MeIm)2 from Heat Capacity Measurements“ J. Am. Chem. Soc. 2020, 142, 4833-4841. doi: 10.1021/jacs.9b13883
F. Topić, T. Friščić* “No regioselectivity for the steroid α-face in cocrystallization of exemestane with aromatic cocrystal formers based on phenanthrene and pyrene“ Can. J. Chem. 2020, 98, 386-393. DOI:10.1139/cjc-2020-0073
H. M. Titi, J.-L. Do, A. J. Howarth, K. Nagapudi, T. Friščić* “Mechanochemical synthesis of metal-organic frameworks using liquid-assisted resonant acoustic mixing (LA-RAM)“ Chem. Sci. 2020, 11, 7578-7584. DOI:10.1039/D0SC00333F (Pick of the Week, RSC World highlight, cover page)
T. Friščić, E. Elaqua, S. Dutta, S. M. Oburn, L. R. MacGillivray* “Total syntheses supramolecular style: solid-state construction of [2.2]cyclophanes with modular control of stereochemistry“ Cryst. Growth Des. 2020, 20, 2584–2589, doi: 10.1021/acs.cgd.9b01712
P. A. Julien, L. S. Germann, H.M. Titi, M. Etter, R. E. Dinnebier, L. Sharma, J. Baltrusaitis*, T. Friščić* “In situ monitoring of mechanochemical synthesis of calcium urea phosphate fertilizer cocrystal reveals highly effective water-based autocatalysis“ Chem. Sci. 2020, 11, 2350-2355. doi: 10.1039/C9SC06224F (cover page)
I. Brekalo, D. Deliz, C. M. Kane, T. Friščić*, K. T. Holman* “Exploring the scope of potential “shoe-last” templates in the mechanochemical synthesis of RHO topology Zeolitic Imidazolate Frameworks (ZIFs)“ Molecules 2020, 25, 633. doi: 10.3390/molecules25030633
I. Huskić, T. Friščić* “From mineralogy to crystal engineering: potential for polymorphism in the metal-organic framework mineral zhemchuzhnikovite and its synthetic analogues“ Cryst. Growth Des. 2020, 20, 525-532. doi: 10.1021/acs.cgd.9b01641
I. Brekalo, W. Yuan, C. Mottillo, Y. Lu, K. T. Holman*, S. L. James*, F. Duarte, P. A. Williams, K. D. M. Harris*, T. Friščić* “Manometric real-time studies of the mechanochemical synthesis of zeolitic imidazolate frameworks“ Chem. Sci. 2020, 11, 2141-2147. doi:10.1039/C9SC05514B
T. Friščić*, C. Mottillo, H. M. Titi “Mechanochemistry for synthesis“ Angew. Chem. Int. Ed. 2020, 59, 1018-1029. doi:10.1002/anie.201906755
I. R. Speight, I. Huskić, M. Arhangelskis, H. M. Titi, R. S. Stein, T. P. Hanusa*, T. Friščić* "Disappearing polymorphs in metal‐organic framework chemistry: unexpected stabilization of a layered polymorph over an interpenetrated 3‐dimensional structure in mercury imidazolate"Chem. Eur. J., 2020, 26, 1811-1818. doi: 10.1002/chem.201905280 (cover page)
L. S. Germann*, A. D. Katsenis, I. Huskić, P. A. Julien, K. Užarević, M. Etter, O. K. Farha, T. Friščić*, R. E. Dinnebier* “Real-time in situ monitoring of particle and structure evolution in mechanochemical synthesis of UiO-66 metal-organic frameworks“ Cryst. Growth Des. 2020, 20, 49-54. doi: 10.1021/acs.cgd.9b01477
F. Hammerer, S. Ostadjoo, T. Friščić*, K. Auclair* “Controlling the reactivity of enzymes in mechanochemistry: inert surfaces protect β-glucosidase activity during ball milling“ ChemSusChem 2020, 13, 106-110. doi:10.1002/cssc.201902752
I. Brekalo, D. Deliz, L. J. Barbour, M. D. Ward, T. Friščić*, K. T. Holman* “Microporosity in a Guanidinium Organodisulfonate Framework“ Angew. Chem. Int. Ed. 2020, 59, 1997-2002. doi:10.1002/anie.201911861
S. Kaabel, T. Friščić*, K. Auclair* “Mechanoenzymatic transformations in the absence of bulk water“ ChemBioChem 2020, 21, 742-758. doi:10.1002/cbic.201900567
2019
G. Ayoub, M. Arhangelskis, X. Zhang, F. Son, T. Islamoglu, T. Friščić*, O. K. Farha* “Air Oxidation of Sulfur Mustard Gas Simulant Using a Pyrene-Based Metal-Organic Framework Photocatalyst“ Beil. J. Nanotech. 2019, 10, 2422-2427. doi:10.3762/bjnano.10.232
B. Karadeniz, D. Žilić, I. Huskić, L. S. Germann, A. M. Fidelli, S. Muratović, I. Lončarić, M. Etter, R. E. Dinnebier, D. Barišić, N. Cindro, T. Islamoglu, O. K. Farha, T. Friščić, K. Užarević* “ Controlling the polymorphism and topology transformation in porphyrinic zirconium metal-organic frameworks via mechanochemistry“ J. Am. Chem. Soc. 2019, 141, 19214-19220. doi:10.1021/jacs.9b10251
S. Ostadjoo, F. Hammerer, T. Friščić*, K. Auclair* “Efficient enzymatic hydrolysis of biomass hemicellulose in the absence of bulk water“ Molecules 2019, 24, 4206 (invited).
F. Topić, K. Lisac, M. Arhangelskis, K. Rissanen*, D. Cinčić, T. Friščić* “Cocrystal trimorphism reveals orthogonality of halogen- and hydrogen-bonds synthons“ Chem. Commun. 2019, 55, 14066-14069. doi:10.1039/C9CC06735C
H. M.Titi, M. Arhangelskis, G. P. Rachiero, T. Friščić*, R. D. Rogers* “Hypergolic Triggers as Cocrystal Formers: Cocrystallization for Creating New Hypergolic Materials with Tunable Energy Content“ Angew. Chem. Int. Ed. 2019, 58, 18399-18404. doi:10.1002/ange.201908690
G. Ayoub, B. Karadeniz, A. J. Howarth, O. K. Farha*, I. Đilović, L. S. Germann, R. E: Dinnebier, K. Užarević*, T. Friščić* “Rational synthesis of microporous mixed-metal metal-organic frameworks with controlled composition using mechanochemistry“ Chem. Mater. 2019, 31, 5494-5501.
J. P. D. Therien, F. Hammerer, T. Friščić*, K. Auclair* “Mechanoenzymatic breakdown of chitinous material to N‐acetylglucosamine: the benefits of a solvent‐less environment“ ChemSusChem 2019, 12, 3481-3490. (cover page) doi:10.1002/cssc.201901310
H. M. Titi, M. Arhangelskis, A. D. Katsenis, C. Mottillo, G. Ayoub, J.-L. Do, A. M. Fidelli, R. D. Rogers*, T. Friščić* “Metal-organic frameworks (MOFs) as fuels for advanced applications: evaluating and modifying the combustion energy of popular MOFs“ Chem. Mater. 2019, 31, 4882-4888.
P. F. Rosen, J. J. Calvin, M. Dickson, A. D. Katsenis, T. Friščić, A. Navrotsky, N. L. Ross, A. I. Kolesnikov, B. F. Woodfield* “Heat capacity and thermodynamic functions of crystalline forms of the metal-organic framework zinc 2-methylimidazolate, Zn(MeIm)2“ J. Chem. Therm. 2019, 136, 160-169.
M. Arhangelskis, A. D. Katsenis, N. Novendra, Z. Akimbekov, D. Gandrath, J. M. Marrett, G. Ayoub, A. J. Morris, O. K. Farha, T. Friščić*, A. Navrotsky* "Theoretical Prediction and Experimental Evaluation of Topological Landscape and Thermodynamic Stability of a Fluorinated Zeolitic Imidazolate Framework" Chem. Mater. 2019, 31, 3777-3783.
G. Ayoub, T. Islamoglu, S. Goswami, T. Friščić*, O. K. Farha* “Torsion angle effect on the activation of UiO metal-organic frameworks (MOFs)“ ACS Appl. Mat. Int. 2019, 11, 15788-15794.
I. Huskić, N. Novendra D.-W. Lim, F. Topić, H. Titi, I. Pekov. S. V. Krivovichev, A. Navrotsky*, H. Kitagawa*, T. Friščić* “Functionality in metal–organic framework minerals: proton conductivity, stability and potential for polymorphism“ Chem. Sci. 2019, 10, 4923-4929.
B. G. Fiss, L. Hatherly, R. S. Stein, T. Friščić*, A. H. Moores* “Mechanochemical Phosphorylation of Polymers and Synthesis of Flame-Retardant Cellulose Nanocrystals“ ACS Sust. Chem. Eng. 2019, 7, 7951-7959.
S. Li, I. Huskić, N. Novendra, H. M. Titi, A. Navrotsky*, T. Friščić* “Mechanochemical synthesis, accelerated aging and thermodynamic stability of the organic mineral paceite and its cadmium analogue“ ACS Omega 2019, 4, 5486-5495 (invited)
I. Huskić, T. Friščić* “Geomimetic approaches in the design and synthesis of metal-organic frameworks: lessons and opportunities for efficient, environmentally-friendly synthesis“ Phil. Trans. Royal Soc. A 2019, DOI:10.1098/rsta.2018.0221 (invited)
H. M. Titi, J. M. Marrett, G. Dayaker, M. Arhangelskis, C. Mottillo, A. J. Morris, G. P. Rachiero, T. Friščić*, R. D. Rogers* “Hypergolic Zeolitic Imidazolate Frameworks (ZIFs) as Next-Generation Solid Fuels: Unlocking the Latent Energetic Behavior of ZIFs“ Sci. Adv. 2019, 5, eaav9044.
S. Kaabel, R. S. Stein, M. Fomitšenko, I. Järving, T. Friščić*, R. Aav* “Size-control by anion templating in mechanochemical synthesis of hemicucurbiturils in the solid state“ Angew. Chem. Int. Ed. 2019, 58, 6230-6234. (VIP paper, cover page) DOI: 10.1002/anie.201813431
D.-K. Bučar*, T. Friščić* “Prof. William Jones and his Materials Chemistry Group: Innovations and Advances in the Chemistry of Solids“ Cryst. Growth Des. 2019, 19, 1479-1487. DOI: 10.1021/acs.cgd.9b00090
E. Colacino*, G. Dayaker, A. Morère, T. Friščić* “Introducing Students to Mechanochemistry via Environmentally Friendly Organic Synthesis Using a Solvent-Free Mechanochemical Preparation of the Antidiabetic Drug Tolbutamide“ J. Chem. Ed. 2019, 96, 766-771. DOI: 10.1021/acs.jchemed.8b00459
K. Lisac, F. Topić, M. Arhangelskis, S. Cepić, P. A. Julien, C. W. Nickels, A. J. Morris, T. Friščić*, D. Cinčić* ”Halogen bonds to phosphorus, arsenic and antimony" Nature Commun. 2019, 10, 61 (voted top 10 Quebec discoveries in 2019 by Quebec Science). DOI:10.1038/s41467-018-07957-6
2018
V. Glembockyte, M. Frenette, C. Mottillo, A. M. Durantini, J. Gostick, V. Štrukil, T. Friščić*, G. Cosa* “Highly photostable and fluorescent microporous solids prepared via solid-state entrapment of BODIPY dyes in a nascent metal-organic framework“ J. Am. Chem. Soc. 2018, 140, 16882-16887.
G. Ayoub, V. Štrukil*, L. Fábián, C. Mottillo, H. Bao, Y. Murata, A. Moores, D. Margetić, M. Eckert-Maksić, T. Friščić* ”Mechanochemistry vs. solution growth: striking differences in bench stability of a cimetidine salt based on a synthetic method" CrystEngComm 2018, 20, 7242-7247. DOI:10.1039/c8ce01727a
I. Huskić, T. Friščić* “Understanding geology through crystal engineering: coordination complexes, coordination polymers and metal-organic frameworks as minerals“ Acta Crystallogr. B 2018, 74, 539-559. (invited) scripts.iucr.org/cgi-bin/paper?S2052520618014762
B. Karadeniz, A. J. Howarth, T. Stolar, T. Islamoglu, I. Dejanović, M. Tireli, S.-Y. Moon, O. K. Farha, T. Friščić, K. Užarević* “Benign by Design: Green and Scalable Synthesis of Zirconium UiO-Metal-Organic Frameworks by Water-Assisted Mechanochemistry“ ACS Sust. Chem. Eng. 2018, 6, 15841-15849.
M. Arhangelskis*, D. B. Jochym, L. Bernasconi, T. Friščić, A. J. Morris*, W. Jones “Time-Dependent Density-Functional Theory for Modelling Solid-State Fluorescence Emission of Organic Multicomponent Crystals" J. Phys. Chem. A 2018, 122, 7514-7521. DOI:10.1021/acs.jpca.8b03481
I. Brekalo, C. Kane, A. Ley, J. Ramirez, T. Friščić*, T. Holman* “Use of a 'Shoe-Last' Solid-State Template in the Mechanochemical Synthesis of High-Porosity RHO-Zinc Imidazolate“ J. Am. Chem. Soc. 2018, 140, 10104-10108.
Y. Zhang, B. E. G. Lucier, S. M. McKenzie, M. Arhangelskis, A. J. Morris, T. Friščić, J. Reid, V. V. Terskikh, Y. Huang* “Welcoming Gallium- and Indium-fumarate MOFs to the Family: Synthesis, Comprehensive Characterization, Observation of Porous Hydrophobicity, and CO2 Dynamics“ ACS Appl. Mat. Int. 2018, 10, 28582-28596.
A. M. Fidelli, B. Karadeniz, A. J. Howarth, I. Huskić,¬ L. S. Germann, I. Halasz, M. Etter, S.-Y. Moon, R. E. Dinnebier, V. Stilinović, O. K. Farha*, T. Friščić*, K. Užarević* ”Green and rapid mechanosynthesis of high-porosity NU- and UiO-type metal–organic frameworks" Chem. Commun. 2018, 54, 6999-7002.
N. Bedeković, V. Stilinović*, T. Friščić, D. Cinčić* ”Comparison of isomeric meta- and para-diiodotetrafluorobenzene as halogen bond donors in crystal engineering" New J. Chem. 2018, 42, 10584-10591 (invited)
S. Mohamed*, A. A. Alwan, A. J. Morris, T. Friščić, A. J. Morris, M. Arhangelskis ”Towards the systematic crystallisation of molecular ionic cocrystals: insights from computed crystal energy landscapes" Faraday Discussions 2018, 211, 401-424.
J. Marrett, C. Mottillo, S. Girard, J.-L. Do, C. W. Nickels, D. Gandrath, L. S. Germann, R. E. Dinnebier, A. J. Howarth, O. K. Farha, T. Friščić,* C.-J. Li* “Supercritical carbon dioxide enables the rapid and scalable conversion of a metal oxide into zeolitic metal–organic frameworks" Cryst. Growth Des. 2018, 18, 3222-3228.
M. Arhangelskis, A. D. Katsenis, A. J. Morris, T. Friščić*, ”Computational evaluation of metal pentazolate frameworks" Chem. Sci. 2018, 9, 3367-3375.
K. Lisac, V. Nemec, F. Topić, M. Arhangelskis, P. Hindle, R. Tran, I. Huskić, T. Friščić*, D. Cinčić* ”Experimental and theoretical investigation of structures, stoichiometric diversity and bench stability of cocrystals with a volatile halogen bond donor" Cryst. Growth Des. 2018, 18, 2387-2396. (invited)
K. Užarević*, N. Ferdelji, T. Mrla, P. A. Julien, B. Halasz, T. Friščić, I. Halasz* ”Enthalpy vs. Friction: Direct measurement and heat flow modelling of unexpected temperature profiles in mechanochemistry of metal-organic frameworks" Chem. Sci. 2018, 9, 2525-2532.
J.-L. Do, D. Tan, T. Friščić* ”Oxidative mechanochemistry for direct conversion of metallic palladium and gold into soluble salts or coordination complexes" Angew. Chem. Int. Ed. 2018, 57, 2667-2671 (highlighted in C&EN, 2018, 96, 8)
C. Mottillo*,T. Friščić “From the benchtop to the pilot plant: making headway in the synthesis of metal-organic frameworks" Chimica Oggi 2018, 36, 44-46 (invited).
F. Hammerer, L.-A. Loots, J.-L. Do, J. P. D. Therien, C. W. Nickels, T. Friščić*, K. Auclair* ”Solvent-free enzyme activity: quick, high-yielding mechano-enzymatic hydrolysis of cellulose into glucose" Angew. Chem. Int. Ed. 2018, 57, 2621-2624.
P. A. Julien, J.-C. Christopherson, H. M. Titi, R. D. Rogers, T. Friščić* ”Investigation of BINOL-3,3’-dicarboxylate as a ligand for the formation of extended coordination-based structures" Supramol. Chem. 2018, 30, 488-503. (invited)
M. Roohnikan, M. Lindner-D’Addario, V. Toader, A. Rey, D. Tan, T. Friščić, L. Reven* “Mechanochemical Nanoparticle Functionalization for Liquid Crystal Nanocomposites Based on COOH-Pyridine Heterosynthons" J. Mat. Chem. C 2018, 6, 1789-1796.
J.-C. Christopherson, F. Topić, C. J. Barrett*, T. Friščić* “Halogen-Bonded Cocrystals as Optical Materials: Next-generation Control over Light-Matter Interactions" Cryst. Growth Des. 2018, 18, 1245-1259.
J. J. Calvin, M. Asplund, Z. Akimbekov, G. Ayoub, A. D. Katsenis, A. Navrotsky, T. Friščić, B. F. Woodfield* “Heat Capacity and Thermodynamic Functions of Crystalline and Amorphous Forms of the Metal Organic Framework Zinc 2-Ethylimidazolate, Zn(EtIm)2 " J. Chem. Thermodynamics 2018, 116, 341-351.
Ziling, D. Tan, T. Friščić, R. Khaliullin* “Why pregnenolone and progesterone, two structurally similar steroids, exhibit remarkably different cocrystallization with aromatic molecules" Phys. Chem. Chem. Phys. 2018, 20, 898-904. DOI:10.1039/C7CP06828J
D. Tan, T. Friščić* “Mechanochemistry for Organic Chemists: An Update" Eur. J. Org. Chem. 2018, 18-33 (invited)
2017
A. Garci, K. J. Castor, J. Fakhoury, J.-L. Do, J. Di Trani, R. S. Stein, A. K. Mittermeier, T. Friščić*, H. Sleiman* “Efficient and Rapid Mechanochemical Assembly of Platinum(II) Squares for Guanine Quadruplex Targeting" J. Am. Chem. Soc. 2017, 139, 16913-16922.
V. Nemec, L. Fotović, T. Friščić, D. Cinčić* “A large family of halogen-bonded cocrystals involving metal-organic building blocks with open coordination sites" Cryst. Growth Des. 2017, 17, 6169-6173 (among top 20 downloads in December)
P. A. Julien, I. Malvestiti, T. Friščić* “The Effect of Milling Frequency on a Mechanochemical Organic Reaction Monitored by In Situ Raman Spectroscopy" Beil. J. Org. Chem. 2017, 13, 2160-2168. (invited)
M. Malca, H. Bao, T. Bastaille, N. K. Saadé, J. M. Kinsella, T. Friščić, A. Moores* “Mechanically activated solvent-free assembly of ultrasmall Bi2S3 nanoparticles: a novel, simple and sustainable means to access chalcogenide nanoparticles" Chem. Mater. 2017, 29, 7766-7773.
M. Malca, P.-O. Ferko, T. Friščić, A. Moores* “Solid-state mechanochemical ω-functionalization of poly(ethylene glycol)” Beil. J. Org. Chem. 2017, 13, 1963-1968.
T. Friščić* “Medicinal Mechanochemistry: from Solid Form Screening to Cleaner and Safer Synthesis of Active Pharmaceutical Ingredients" Chimica Oggi, 2017, 35, 27-30. (invited)
J.-L. Do, T. Friščić* "Towards Chemistry 2.0: Developing a New, Solvent-free System of Chemical Synthesis Based on Mechanochemistry" Synlett 2017, 28, 2066-2092.
S. Lukin, T. Stolar, M. Tireli, M. V. Blanco, D. Babić, T. Friščić, K. Užarević*, I. Halasz* "Tandem in situ monitoring for quantitative assessment of mechanochemical reactions involving structurally unknown phases" Chem. Eur. J. 2017, 23, 13941-13949.
P. A. Julien*, C. Mottillo, T. Friščić* “Metal-organic frameworks meet scalable and sustainable synthesis" Green Chem. 2017, 19, 2729-2747.
Z. Akimbekov, A. D. Katsenis, G. P. Nagabushana, G. Ayoub, M. Arhangelskis, A. J. Morris, T. Friščić*, A. Navrotsky* “Experimental and theoretical evaluation of the stability of true MOF polymorphs explains their mechanochemical interconversions" J. Am. Chem. Soc. 2017, 139, 7952-7957.
T. Stolar, L. Batzdorf, S. Lukin, D. Žilić, C. Mottillo, T. Friščić, F. Emmerling*, I. Halasz*, K. Užarević* “In situ monitoring of mechanosynthesis of the archetypal metal-organic framework HKUST-1: effect of liquid additives on the milling reactivity" Inorg. Chem. 2017, 56, 6599-6608.
J.-C. Christopherson, K. P. Potts, O. S. Bushuyev, F. Topić, I. Huskić, K. Rissanen, C. J. Barrett*, T. Friščić* “Assembly and dichroism of a four-component halogen-bonded metal-organic cocrystal salt solvate involving dicyanoaurate(I) acceptors" Faraday Discuss. 2017, 203, 441-457.
M. Glavinović, M. Krause, L. Yang, J. A. McLeod, L. Liu, K. M. Baines*, T. Friščić*, J.-P. Lumb* “A Chlorine-Free Protocol for Processing Germanium" Science Adv. 2017, 3, e1700149.
A. Margariti, S. Rapti, A. D. Katsenis, T. Friščić, Y. Georgiou, M. J. Manos*, G. S. Papaefstathiou* "Cu2+ sorption from aqueous media by a recyclable Ca2+ framework” Inorg. Chem. Front. 2017, 4, 773-781.
C. Mottillo*, T. Friščić* “Advances in the solid-state transformations of coordination bonds: from the ball mill to the aging chamber" Molecules 2017, 22, 144. DOI:10.3390/molecules22010144
J.-L. Do, T. Friščić* “Mechanochemistry: A Force of Synthesis" ACS Central Science 2017, 3, 13-19.
D. Tan, T. Friščić* “Carbodiimide insertion into sulfonimides: one-step route to azepine derivatives via a two-atom saccharin ring expansion" Chem. Commun. 2017, 53, 901-904.
2016
Y. X. Shi, K. Xu, J. K. Clegg, R. Ganguly, H. Hirao, T. Friščić, F. García* “The First Synthesis of the Sterically Encumbered Adamantoid Phosphazane P4(NtBu)6: Enabled by Mechanochemistry" Angew. Chem. Int. Ed. 2016, 55, 12736-12740.
I. Huskić, I. Pekov, S. Krivovichev,* T. Friščić* "Minerals with Metal-Organic Framework Structures" Science Advances 2016, 2, e1600621.
M. J. Rak, T. Friščić, A. Moores* "One-step, solvent-free mechanosynthesis of silver nanoparticle-infused lignin composites for use as highly active multidrug resistant antibacterial filters" RSC Advances 2016, 6, 58365-58370.
O. S. Bushuyev, T. Friščić*, C. J. Barrett* "Photo-induced motion of azo dyes in organized media: from single and liquid crystals, to MOFs and machines" CrystEngComm 2016, 18, DOI:10.1039/C6CE01128D
R. Banerjee, G. M. Day, T. Friščić, H. Zhang "2016 New talent: crystal engineering at its biggest and strongest" CrystEngComm 2016, 18, 3963-3967.
D. Tan, L. Loots, T. Friščić* "Towards medicinal mechanochemistry: evolution of milling from pharmaceutical solid form screening to the synthesis of active pharmaceutical ingredient (APIs)" Chem. Commun. 2016, 52, 7760-7781.
I. Huskić, J.-C. Christopherson, K. Užarević*, T. Friščić* "In situ monitoring of vapour-induced assembly of pharmaceutical cocrystals using a benchtop powder X-ray diffractometer" Chem. Commun. 2016, 52, 5120-5123.
K. Užarević,* V. Štrukil, C. Mottillo, P. A. Julien, A. Puškarić, T. Friščić,* I. Halasz* " Exploring the effect of temperature on a mechanochemical reaction by in situ synchrotron powder X-ray diffraction" Cryst. Growth Des. 2016, 16, 2342-2347.
P. A. Julien, K. Užarević, A. D. Katsenis, S. A. J. Kimber, T. Wang, O. K. Farha, Y. Zhang, J. Casaban, L. Germann, M. Etter, R. E. Dinnebier, S. L. James*, I. Halasz*, T. Friščić* "In situ monitoring and mechanism of the mechanochemical formation of a microporous MOF-74 framework" J. Am. Chem. Soc. 2016, 138, 2929-2932.
K. Korpany, C. Mottillo, J. Balchelder, P. Dong, S. Trudel, T. Friščić*, A. S. Blum* "One-step ligand exchange and switching from hydrophobic to water-stable hydrophilic superparamagnetic iron oxide nanoparticles by mechanochemical milling" Chem. Commun. 2016, 52, 3054-3057.
O. S. Bushuyev, A. Tomberg, J. R. Vinden, N. Moitessier, C. J. Barrett*, T. Friščić* "Azo···phenyl stacking: a persistent self-assembly motif guides the assembly of fluorinated cis-azobenzenes into photo-mechanical needle crystals" Chem. Commun. 2016, 52, 2103-2106. (invited)
K. Užarević, T. C. Wang, S.-Y. Moon, A. M. Fidelli, J. T. Hupp, O. K. Farha*, T. Friščić* "Mechanochemical and solvent-free synthesis of zirconium-based metal-organic frameworks", Chem. Commun. 2016, 52, 2133-2136.
M. Glavinovic, F. Qi, A. D. Katsenis, T. Friščić*, J.-P. Lumb* "Redox-promoted associative assembly of metal-organic materials" Chem. Sci. 2016, 7, 707-712.
O. S. Bushuyev, C. J. Barrett*, T. Friščić* "Controlling Dichroism of Molecular Crystals by Cocrystallization" Cryst. Growth Des. 2016, 16, 541-545.
2015
K. Užarević, I. Halasz, T. Friščić* "Real-time and in situ monitoring of mechanochemical reactions: a new playground for all chemists" J. Phys. Chem. Lett. 2015, 6, 4129-4140.
V. Štrukil*, D. Gracin, O. V. Magdysyuk, R. E. Dinnebier, T. Friščić* "Trapping reactive intermediates by mechanochemistry: elusive aryl N-thiocarbamoylbenzotriazoles as bench-stable reagents" Angew. Chem. Int. Ed. 2015, 54, 8440-8443.
J. G. Hernández, T. Friščić* "Metal-catalyzed organic reactions using mechanochemistry" Tetrahedron Letters 2015, 56, 4253-4265.
C. Mottillo, T. Friščić* "Supramolecular imidazolium frameworks: direct analogues of metal azolate frameworks with a charge-inverted node-and-linker structure" Chem. Commun. 2015, 51, 8924-8927. (back journal cover)
T. Friščić*, S. L. James, E. V. Boldyreva, C. Bolm, W. Jones, J. Mack, J. W. Steed, K. S. Suslick "Highlights from Faraday discussion 170: Challenges and opportunities of modern mechanochemistry, Montreal, Canada, 2014" Chem. Commun. 2015, 51, 6248-6256.
A. D. Katsenis, A. Puškarić, V. Štrukil, C. Mottillo, P. A. Julien, K. Užarević, M.-H. Pham, T.-O. Do, S. A. J. Kimber, P. Lazić, O. Magdysyuk, R. E. Dinnebier, I. Halasz,*, T. Friščić* "In situ X-ray diffraction monitoring of a mechanochemical reaction reveals a unique-topology metal-organic framework" Nature Commun. 2015 6:6662.
J.-L. Do, C. Mottillo, D. Tan, V. Štrukil, T. Friščić* "Mechanochemical ruthenium-catalysed olefin metathesis" J. Am. Chem. Soc. 2015, 137, 2476-2479.
K. J. Ardila-Fierro, V. André, D. Tan, M. T. Duarte, R. W. Lancaster, P. G. Karamertzanis, T. Friščić* "Molecular recognition of steroid hormones in the solid state: stark differences in cocrystallization of β-estradiol and estrone" Cryst. Growth Des. 2015, 15, 1492-1501.
D. Prochowicz, K. Sokołowski, I. Justyniak, A. Kornowicz, D. Fairen-Jimenez, T. Friščić, J. Lewinski* "A mechanochemical strategy for IRMOFs assembly based on pre-designed oxo-zinc precursors" Chem. Commun. 2015, 51, 4032-4035.
O. S. Bushuyev, D. Tan, C. J. Barrett,* T. Friščić* "Fluorinated azobenzenes with highly strained geometries for halogen bond-driven self-assembly" CrystEngComm 2015, 17, 73-80.
2014
D. Cinčić,* T. Friščić "Synthesis of an extended halogen-bonded metal-organic structure in a one-pot mechanochemical reaction that combines covalent, coordination and supramolecular synthesis" CrystEngComm 2014, 16, 10169-10172.
T. Friščić, C. B. Aakeröy "International year of crystallography celebration: North America" CrystEngComm 2014, 16, 7160-7161.
Y. Fang, N. Salamé, S. Woo, D. S. Bohle, T. Friščić*, L. A. Cuccia* "Rapid and facile solvent-free mechanosynthesis in a cell lysis mill: preparation and mechanochemical complexation of aminobenzoquinones" CrystEngComm 2014, 16, 7180-7185.
J. G. Hernández, I. S. Butler*, T. Friščić* "Multi-step and multi-component organometallic synthesis in one pot using orthogonal mechanochemical reactions" Chem. Sci. 2014, 5, 3576-3582.
O. S. Bushuyev, T. C. Corkery, C. J. Barrett*, T. Friščić* "Photo-mechanical azobenzene co-crystals and in situ X-ray diffraction study of their optically-induced crystal-to-crystal isomerization" Chem. Sci. 2014, 5, 3158-3164. (highlighted in an article by Chemistry World.
D. Tan, C. Mottillo, A. D. Katsenis, V. Štrukil, T. Friščić* "Development of a New C-N Coupling using Mechanochemistry: Catalytic Coupling of Arylsulfonamides and Carbodiimides" Angew. Chem. Int. Ed. 2014, 53, 9321-9324.
C. Mottillo, T. Friščić* "Carbon dioxide sensitivity of zeolitic imidazolate frameworks" Angew. Chem. Int. Ed. 2014, 53, 7471-7474.
M. J. Rak, T. Friščić, A. H. Moores* "Mechanochemical synthesis of Au, Pd, Ru and Re nanoparticles with lignin as a bio-based reducing agent and stabilizing matrix" Faraday Discuss. 2014, 170, 155-167.
D. Gracin, V. Štrukil, T. Friščić, I. Halasz*, K. Užarević* "Laboratory real-time and in situ monitoring of mechanochemical milling reactions using Raman spectroscopy" Angew. Chem. Int. Ed. 2014, 53, 6193-6197.
I. Halasz,* T. Friščić*, S. A. J. Kimber, K. Užarević, A. Puškarić, C. Mottillo, P. Julien, V. Štrukil, V. Honkimäki and R. E. Dinnebier "Quantitative in situ and real-time monitoring of mechanochemical reactions" Faraday Discuss. 2014, 170, 203-221.
J. G. Hernández, N. A. J. Macdonald, C. Mottillo, I. S. Butler* and T. Friščić* "A mechanochemical strategy for oxidative addition: remarkable yields and stereoselectivity in the halogenation of organometallic Re(I) complexes" Green Chem. 2014, 16, 1087-1092.
D. Tan, V. Štrukil, C. Mottillo, T. Friščić* "Mechanosynthesis of pharmaceutically relevant sulfonyl-(thio)ureas" Chem. Commun. 2014, 50, 5248-5250. (invited for the 2014 Emerging Investigator theme issue)
M. J. Rak, N. K. Saade, T. Friščić and A. Moores* "Mechanosynthesis of Ultra-small Monodisperse Amine-Stabilized Gold Nanoparticles with Controllable Size" Green Chem. 2014, 16, 86-89.
F. Qi, R. Stein, T. Friščić* "Mimicking mineral neogenesis for the clean synthesis of metal-organic materials from mineral feedstocks: coordination polymers, MOFs and metal oxide separation" Green Chem. 2014, 16, 121-132 (hot article).
2013
O. S. Bushuyev, A. Tomberg, C. J. Barrett*, T. Friščić* "Shaping Crystals with Light: Crystal-to-Crystal cis-trans Isomerization and Photomechanical Effect in Fluorinated Azobenzenes" J. Am. Chem. Soc. 2013, 135, 12556-12559.
M. Sacchi, A. Brewer, S. Jenkins, J. Parker, T. Friščić, S. M. Clarke* "Combined diffraction and DFT calculations of halogen bonded co-crystal monolayers" Langmuir 2013, 29, 14903-14911.
I. Halasz, A. Puškarić, S. A. J. Kimber, P. J. Beldon, A. M. Belenguer, F. Adams, V. Honkimäki, R. E. Dinnebier, B. Patel, W. Jones, V. Štrukil, T. Friščić* "Real-time in situ X-ray diffraction monitoring of mechanochemical transformations of pharmaceutical cocrystals" Angew. Chem. Int. Ed. 2013, 52, 11538-11541 (inside cover).
S. L. James,* T. Friščić* "Mechanochemistry" Chem. Soc. Rev. 2013, 42, 7494-7496.
S. L. James* and T. Friščić* "Mechanochemistry: a web themed issue" Chem. Commun. 2013, 49, 5349-5350.
I. Halasz, S. A. J. Kimber, P. J. Beldon, A. M. Belenguer, F. Adams, V. Honkimäki, R. C. Nightingale, R. E. Dinnebier, T. Friščić* "In situ and real time monitoring of mechanochemical milling reactions using synchrotron X-ray diffraction" Nature Protocols 2013, 8, 1718-1729 (invited).
C. Mottillo, Y. Lu, M.-H. Pham, M. J. Cliffe, T.-O. Do, T. Friščić* "Mineral neogenesis as an inspiration for mild, solvent-free synthesis of bulk microporous metal–organic frameworks from metal (Zn, Co) oxides" Green Chemistry 2013, 15, 2121-2131 (hot article).
M. Frenette, G. Cosa*, T. Friščić* "Characterization of organic solid forms and real-time in situ monitoring of their transformations using solid-state fluorescence" CrystEngComm 2013, 15, 5100-5106.
T. Friščić*, I. Halasz, P. J. Beldon, A. M. Belenguer, F. Adams, S. A. J. Kimber, V. Honkimäki, R. E. Dinnebier "Real-time and in situ monitoring of mechanochemical reactions" Nature Chemistry, 2013, 5, 66-73. Highlighted in Chemical & Engineering News: http://cen.acs.org/articles/90/i49/X-Ray-Vision-Mechanochemical-Mills.html; also highlighted by: the UK Science & Technology Facilities Council, European Synchrotron Research Facility; McGill University; Canadian Chemical News and a number of news outlets.
J. Galcera*, T. Friščić, E. Molins, W. Jones "Isostructurality in three-component crystals achieved by the combination of persistent hydrogen bonding motifs and solvent inclusion" CrystEngComm, 2013, 15, 1332-1338.
A. Y. Brewer, T. Friščić, L. M. Overvoorde, J. E. Parker, C. Richardson, S. M. Clarke* "The monolayer structure of 1,2-di(4-pyridyl)ethylene physisorbed on a graphite surface" Mol.Phys. 2013, 111, 73-79.
2012
M. D. Eddleston, M. Arhangelskis, T. Friščić, W. Jones* "Solid state grinding as a tool to aid enantiomeric resolution by cocrystallisation" Chem. Commun. 2012, 48, 11340-11342.
V. Štrukil, M. D. Igrc, M. Eckert-Maksić,* T. Friščić* "Desymmetrisation of aromatic diamines and synthesis of non-symmetrical thiourea derivatives by click-mechanochemistry" Chem. Commun. 2012, 48, 9705-9707.
V. Štrukil, M. D. Igrc, L. Fábián, M. Eckert-Maksić,* S. L. Childs, D. G. Reid, M. J. Duer, I. Halasz, C. Mottillo, T. Friščić* "A model for a solvent-free synthetic organic research laboratory: click-mechanosynthesis and structural characterization of thioureas without bulk solvents" Green Chem. 2012, 14, 2462-2473 (journal cover).
J. Galcera,* T. Friščić, K. E. Heyczik, L. Fábián, S. M. Clarke, G. M. Day, E. Molins, W. Jones* "Isostructural organic binary-host frameworks with tuneable and diversely decorated inclusion cavities" CrystEngComm 2012, 14, 7898-7906 (journal cover).
M. J. C. Cliffe, C. Mottillo, R. S. Stein, D.-K. Bučar, T. Friščić* "Accelerated aging: a low energy, solvent-free alternative to solvothermal and mechanochemical synthesis of metal-organic materials" Chem. Sci. 2012, 3, 2495-2500. (highlighted on the RSC Chemical Science Blog and www.chemeurope.com, see: Accelerated aging to make mofs and Organic accelerated aging to make mofs.
S. Y. Oh, C. W. Nickels, F. Garcia, W. Jones,* T. Friščić* "Switching between halogen- and hydrogen-bonding in stoichiometric variations of a cocrystal of a phosphine oxide" CrystEngComm 2012, 14, 6110-6114. (invited, journal cover, hot article, highlighted on
I. Huskić, I. Halasz,* T. Friščić, H. Vančik "Mechanosynthesis of nitrosobenzenes: a proof-of-principle study in combining solvent-free synthesis with solvent-free separations" Green Chem. 2012,14, 1597-1600.
V. Štrukil, M. D. Igrc, M. Eckert-Maksić*, T. Friščić* "Click mechanochemistry: quantitative synthesis of chiral organocatalysts by efficient two-fold thiourea coupling on vicinal diamines" Chem. Eur. J. 2012, 18, 8464-8473. (included in Wiley-VCH Hot Topics selection for Click Chemistry
T. Friščić* "Supramolecular concepts and new techniques in mechanochemistry: cocrystals, cages, rotaxanes, open metal-organic materials" Chem. Soc. Rev. 2012, 41, 3493-3510 (invited).
T. Friščić*, I. Halasz, V. Štrukil, M. Eckert-Maksić, R. E. Dinnebier "Clean and efficient synthesis using mechanochemistry: coordination polymers, open metal-organic frameworks and metallodrugs" Croat. Chem. Acta 2012, 85, 367-378 (invited).
A. Delori, T. Friščić, W. Jones* "The role of mechanochemistry in the development of pharmaceutical materials based on supramolecular designs" CrystEngComm 2012, 14, 2350-2362 (hot article).
D. Yan, A. Delori, G. O. Lloyd, B. Patel, T. Friščić, G. M. Day, D.-K. Bučar, W. Jones,* J. Lu, M. Wei, D. G. Evans, X. Duan, "Modification of luminescent properties of a coumarin derivative by formation of multi-component crystals" CrystEngComm 2012, 14, 5121-5123.
S. L. James, C. J. Adams, C. Bolm, D. Braga, P. Collier, T. Friščić, F. Grepioni, K. D. M. Harris, G. Hyatt, W. Jones, A. Krebs, J. Mack, L. Maini, A. G. Orpen, I. P. Parkin, W. C. Shearouse, J. W. Steed, D. Waddell "Mechanochemistry: opportunities for new and cleaner synthesis" Chem. Soc. Rev. 2012, 41, 413-447.
E. Elacqua, T. Friščić, L. R. MacGillivray* "[2.2]Paracyclophane as a Target of the Organic Solid State: Emergent Properties via Supramolecular Construction" Isr. J. Chem. 2012, 52, 53-59.
2011
D. Yan, A. Delori, G. O. Lloyd, T. Friščić, G. M. Day, W. Jones,* J. Lu, M. Wei, D. G. Evans, X. Duan "A Cocrystal Strategy to Tune the Luminescent Properties of Stilbene-Type Organic Solid-State Materials" Angew. Chem. Int. Ed. 2011, 50, 12483-12486. (highlighted in Nature Chemistry: J. Wuest, Nature Chem., 2012, 4, 74-75).
T. D. Bennett, S. Cao, J. C. Tan, D. A. Keen, E. G. Bithell, P. J. Beldon, T. Friščić, A, K. Cheetham* "Facile Mechanosynthesis of Amorphous Zeolitic Imidazolate Frameworks" J. Am. Chem. Soc. 2011, 133, 14546-14549.
T. Friščić*, G. M. Day* "Dynamic behaviour in the solid state" CrystEngComm 2011, 13, 4303.
V. M. André, A. Hardeman, I. Halasz, R. S. Stein, G. J. Jackson, D. G. Reid, M. J. Duer, C. Curfs, M. T. Duarte, T. Friščić* "Mechanosynthesis of the Metallodrug Bismuth Subsalicylate from Bi2O3 and Structure of a Bismuth Salicylate without Auxiliary Organic Ligands" Angew. Chem. Int. Ed. 2011, 50, 7858–7861.
C. Karunatilaka, D.-K. Bučar, L. R. Ditzler, T. Friščić, L. R. MacGillivray,* A. V. Tivanski* "Softening and hardening of macro- and nano-sized organic cocrystals in a single-crystal transformation" Angew. Chem. Int. Ed. 2011, 50, 8642-8646.
L. R. MacGillivray,* M. B. Atkinson, S. Mariappan, D.-K. Bučar, J. Baltrusaitis, T. Friščić, N. Sinada "Crystal engineering rescues a solution organic synthesis in a cocrystallization confirms the configuration of a molecular ladder" Proc. Natl. Acad. Sci. USA 2011, 108, 10974-10979.
(F) T. Friščić, D. G. Reid, G. M. Day, M. J. Duer and W. Jones* "Effect of Fluorination on Molecular Conformation in the Solid State: Tuning the Conformation of Cocrystal Formers" Cryst. Growth Des. 2011, 11, 972-981. Highlighted on the ACS Crystal Growth and Design network page:
T. Friščić*, I. Halasz, F. C. Strobridge, R. E. Dinnebier, R. S. Stein, L. Fábián, C. Curfs "A rational approach to screen for hydrated forms of the pharmaceutical derivative magnesium naproxen using liquid-assisted grinding" CrystEngComm 2011, 13, 3125-3129.
A. M. Belenguer*, T. Friščić*, G. M. Day, J. K. M. Sanders "Solid-state dynamic combinatorial chemistry: reversibility and thermodynamic product selection in covalent mechanosynthesis" Chem. Sci. 2011, 2, 696-700.
S. M. Clarke*, T. Friščić, W. Jones, A. Mandal, C. Sun and J. E. Parker "Observation of a two-dimensional halogen-bonded cocrystal at sub-monolayer coverage using synchrotron X-ray diffraction" Chem. Commun. 2011, 47, 2526-2528.
S. M. Clarke*, T. Friščić, A. Mandal, C. Sun and J. E. Parker "Monolayer structure of 4,4’-bipyridine on graphite at sub-monolayer coverage" Mol. Phys. 2011, 109, 477-481.
D. Cinčić, T. Friščić*, W. Jones* "Experimental and database studies of three-centered halogen bonds with bifurcated acceptors present in molecular crystals, cocrystals and salts" CrystEngComm 2011, 13, 3224-3231 (invited).
M. T. Neary, D. G. Reid, M. J. Mason, T. Friščić, M. J Duer,* M. Cusack "Contrasts between organic participation in apatite biomineralization in brachiopod shell and vertebrate bone identified by nuclear magnetic resonance spectroscopy” J. R. Soc. Interface 2011, 8, 282-288.
2010
P. J. Beldon, L. Fábián, R. S. Stein, A. Thirumurugan, A. K. Cheetham, T. Friščić* "Rapid room-temperature synthesis of zeolitic imidazolate frameworks using mechanochemistry" Angew. Chem. Int. Ed. 2010, 49, 9640-9643.
A. Blagus, D. Cinčić, T. Friščić, B. Kaitner,* V. Stilinović "Schiff bases derived from hydroxyaryl aldehydes: molecular and crystal structure, tautomerism, quinoid effect, coordination compounds" Maced. J. Chem. Chem. Eng. 2010, 29, 117-138.
V. Štrukil, L. Fábián, D. G. Reid, M. J. Duer, G. J. Jackson, M. Eckert-Maksić,* T. Friščić* "Towards an environmentally-friendly laboratory: dimensionality and reactivity in the mechanosynthesis of metal-organic compounds" Chem. Commun. 2010, 46, 9191-9193.
S. Karki, L. Fábián, T. Friščić and W. Jones* "New solid forms of artemisinin obtained through cocrystallisation" CrystEngComm 2010, 12, 4038-4041. Highlighted on the ACS Crystal Growth and Design network page.
J. Bradley, L. Bridgland, D. Colyer, M. J. Duer,* T. Friščić, J. Gallagher, D. G. Reid, J. Skepper, C. Trasler "NMR of biopolymer-apatite composites: Developing a model of the molecular structure of the mineral-matrix interface in calcium phosphate biomaterials" Chem. Mater. 2010, 22, 6109-6116.
E. H. H. Chow, F. C. Strobridge, T. Friščić* "Mechanochemistry of magnesium oxide revisited: facile derivatisation of pharmaceuticals using coordination and supramolecular chemistry" Chem. Commun. 2010, 46, 6368-6370.
T. Friščić* "New opportunities for materials synthesis using mechanochemistry" J. Mat. Chem. 2010, 20, 7599-7605.
T. Friščić*, R. W. Lancaster, L. Fábián, P. G. Karamertzanis* "Tunable recognition of the steroid α-face by adjacent π-electron density" Proc. Natl. Acad. Sci. USA 2010, 107, 13216-13221.
F. C. Strobridge, N. Judaš, T. Friščić* "A stepwise mechanism and the role of the liquid phase in the liquid-assisted grinding synthesis of metal-organic materials" CrystEngComm 2010, 12, 2409-2418 (invited).
T. Friščić, W. Jones* "Benefits of cocrystallisation in pharmaceutical materials science: An update" J. Pharm. Pharmacol. 2010, 62, 1547-1559 (invited).
G. Lapadula, N. Judaš, T. Friščić*, W. Jones* "A three-component modular strategy to extend and link coordination complexes using halogen bonds to O-, S- and π-acceptors" Chem. Eur. J. 2010, 16, 7400-7403.
W. Yuan*, T. Friščić*, D. Apperley, S. L. James* "High reactivity of metal-organic frameworks under grinding conditions - parallels with organic molecular materials" Angew. Chem. Int. Ed. 2010, 49, 3916-3919.
A. J. Cruz-Cabeza, S. Karki, L. Fábián, T. Friščić, G. M. Day, W. Jones* "Predicting Stoichiometry and Structure of Solvates" Chem. Commun. 2010, 46, 2224-2226.
T. Friščić*, D. G. Reid, I. Halasz, R. S. Stein, R. E. Dinnebier, M. J. Duer "Ion- and liquid-assisted grinding: improved mechanochemical synthesis of metal-organic frameworks reveals salt inclusion and anion templating" Angew. Chem. Int. Ed. 2010, 49, 712-715. Highlighted as an Angewandte Chemie "Hot Paper"
2009
T. Friščić, W. Jones "Three-component molecular assembly using mechanochemical grinding" Annales de Chimie: Science des Matériaux 2009, 34, 415-428 (invited).
T. Friščić*, E. Meštrović*, D. Škalec-Šamec, B. Kaitner, L. Fábián " One-pot mechanosynthesis with three levels of molecular self-assembly: coordination bonds, hydrogen bonds and host-guest inclusion" Chem. Eur. J. 2009, 15, 12644-12652.
T. Friščić*, L. Fábián "Mechanochemical conversion of a metal oxide into coordination polymers and porous frameworks using liquid-assisted grinding (LAG)" CrystEngComm 2009, 11, 743-745.
T. Friščić*, S. L. Childs*, S. A. A. Rizvi, W. Jones "The role of solvent in mechanochemical and sonochemical cocrystal formation: a solubility-based approach for predicting cocrystallisation outcome" CrystEngComm 2009, 11, 418-426 (invited).
S. Karki, T. Friščić, L. Fábián, P. R. Laity, G. M. Day, W. Jones* "Improving mechanical properties of crystalline solids by cocrystal formation: new compressible forms of paracetamol" Adv. Mater. 2009, 21, 3905-3909. Invited, highlighted in Chemistry & Engineering News, July 27, 2009, p.46.
T. Friščić, L. R. MacGillivray* " Engineering cocrystal and polymorph architecture via pseudoseeding" Chem. Commun. 2009, 773-775.
E. P. J. Parrott, J. A. Zeitler, T. Friščić, M. Pepper, W. Jones, G. M. Day*, L. F. Gladden* "Testing the sensitivity of terahertz spectroscopy to changes in molecular and supramolecular structure: a study of structurally similar cocrystals" Cryst. Growth Des. 2009, 9, 1452-1460.
T. Friščić, W. Jones* "Recent advances in understanding the mechanism of cocrystal formation via grinding" Cryst. Growth Des. 2009, 9, 1621-1637 (invited).
S. Karki, T. Friščić, W. Jones* "Control and interconversion of cocrystal stoichiometry by grinding: stepwise mechanism for the formation of a hydrogen-bonded cocrystal" CrystEngComm 2009, 11, 470-481 (invited).
M. J. Duer*, T. Friščić, R. C. Murray, D. G. Reid and E. R. Wise "The Mineral Phase of Calcified Cartilage: its Molecular Structure and Interface with the Organic Matrix" Biophysical Journal 2009, 96, 3372-3378.
2008
T. D. Hamilton, G. S. Papaefstathiou, T. Friščić, D.-K. Bučar, L. R. MacGillivray* "Onion-Shell Metal-Organic Polyhedra (MOPs): A General Approach to Decorate the Exteriors of MOPs using Principles of Supramolecular Chemistry" J. Am. Chem. Soc. 2008, 130, 14366-14367.
M. B. J. Atkinson, D. K. Bučar, A. N. Sokolov, T. Friščić, C. Robinson, M. Bilal, N. G. Sinada, A. Chevannes, L. R. MacGillivray* "General application of mechanochemistry to templated solid-state reactivity: rapid and solvent-free access to crystalline supermolecules" Chem. Commun. 2008, 5713-5715.
D. Cinčić, T. Friščić, W. Jones* "Structural Equivalence of Br and I Halogen Bonds: A Route to Isostructural Materials with Controllable Properties” Chem. Mater. 2008, 20, 6623-6626.
M. J. Duer*, T. Friščić, D. Proudfoot, D. G. Reid, M. Schoppet, C. M. Shanahan, J. N. Skepper, E. R. Wise "The mineral surface in calcified plaque is like that of bone - Further evidence for regulated mineralization" Arter. Thromb. Vasc. Biol. 2008, 28, 2030-2034.
J. R. Harjani, T. Friščić, L. R. MacGillivray, R. D. Singer* "Removal of Metal Ions from Aqueous Solutions Using Chelating Task-Specific Ionic Liquids" Dalton Trans. 2008, 4595-4601.
D. Cinčić, T. Friščić, W. Jones* "A cocrystallisation-based strategy to construct isostructural solids" New J. Chem. 2008, 32, 1776-1781.
D. J. Berry, C. C. Seaton, W. Clegg, R. W. Harrington, S. J. Coles, P. N. Horton, M. B. Hursthouse, R. Storey, W. Jones, T. Friščić, N. Blagden* "Applying hot-stage microscopy to co-crystal screening: A study of nicotinamide with seven active pharmaceutical ingredients" Cryst. Growth Des. 2008, 8, 1697-1712.
D. Cinčić, T. Friščić, W. Jones* "Stepwise mechanism for the mechanochemical synthesis of halogen-bonded cocrystal architectures " J. Am. Chem. Soc. 2008, 130, 7524-7525.
T. Friščić, L. Fábián, J. C. Burley, D. G. Reid, M. J. Duer, W. Jones* "Exploring the relationship between cocrystal stability and symmetry: Is Wallach's rule applicable to multi-component solids?" Chem. Commun. 2008, 1644-1646.
T. Friščić, A. V. Trask, W. Jones,* W. D. S. Motherwell "Guest-directed assembly of caffeine and succinic acid into topologically different heteromolecular host networks upon grinding" Cryst. Growth Des. 2008, 8, 1605-1609.
L. R. MacGillivray,* G. S. Papaefstathiou, T. Friščić, T. D. Hamilton, D.-K. Bučar, Q. Chu, D. B. Varshney, I. G. Georgiev "Supramolecular control of reactivity in the solid-state: from templates to ladderanes to metal-organic frameworks" Acc. Chem. Res. 2008, 41, 280-291.
T. Friščić, L. Klasinc,* B. Kovač, L. R. MacGillivray* "HeI photoelectron spectra and gas-phase electronic structures of end-functionalised [3]- and [5]-ladderanes" J. Phys. Chem. B 2008, 112, 1493-1496.
D. Cinčić, T. Friščić, W. Jones* "Isostructural materials achieved via structurally equivalent donors and acceptors in halogen-bonded cocrystals" Chem. Eur. J. 2008, 14, 747-753.
2007
S. Karki, L Fábián, T. Friščić, W. Jones* "Powder X-ray diffraction: An emerging method to structurally characterize organic solids" Org. Letters. 2007, 9, 3133-3136.
S. Karki, T. Friščić, W. Jones,* W. D. S. Motherwell "Solid-state synthesis of pharmaceutical cocrystals and cocrystal hydrates via neat and liquid-assisted grinding" Mol. Pharm. 2007, 4, 347-354 (invited).
K. L. Nguyen, T. Friščić, G. M. Day, L. F. Gladden, W. Jones* "Terahertz time-domain spectroscopy and the quantitative monitoring of mechanochemical cocrystal formation" Nature Materials 2007, 6, 206-209.
T. Friščić, W. Jones* "Cocrystal architecture and properties: design and building of chiral and racemic structures by solid-solid reactions" Faraday Discussions 2007, 136, 161-172.
J. R. Harjani, T. Friščić, L. R. MacGillivray, R. D. Singer* "Metal chelate formation using a task-specific ionic liquid" Inorg. Chem. 2007, 45 10025-10027.
2006
T. Friščić, L. Fábián, J. C. Burley, W. Jones,* W. D. S. Motherwell "Exploring cocrystal-cocrystal reactivity via liquid-assisted grinding: assembling of racemic and dismantling of enantiomeric cocrystals" Chem. Commun. 2006, 5009-5011.
T. Friščić, A. V. Trask, W. Jones,* W. D. S. Motherwell "Screening for inclusion compounds and systematic construction of three-component solids via liquid-assisted grinding" Angew. Chem. Int. Ed. 2006, 45, 7546-7550.
A. N. Sokolov, T. Friščić, S. Blais, J. A. Ripmeester, L. R. MacGillivray* "Persistent one-dimensional face-to-face π-stacks within organic cocrystals" Cryst. Growth Des. 2006, 6, 2427-2428.
T. Friščić, L. R. MacGillivray* "First step in the template-controlled solid-state synthesis of a paracyclophane: A single-crystal-to-single-crystal reaction involving a finite supramolecular assembly" Aust. J. Chem. 2006, 59, 613-616.
T. Friščić, L. R. MacGillivray* "Modularity in organic solid-state and supramolecular chemistry" Croat. Chem. Acta. 2006, 79, 327-333.
A. N. Sokolov, T. Friščić, L. R. MacGillivray* "Enforced face-to-face stacking of organic semiconductor building blocks within hydrogen-bonded molecular co-crystals" J. Am. Chem. Soc. 2006, 128, 2806-2807.
T. Friščić, L. R. MacGillivray* "Increasing the landscape of structural motifs in co-crystals of resorcinols with ditopic aromatics: a one-dimensional π-stacked hydrogen-bonded polymer involving a phenanthroline" Mol. Cryst. Liq. Cryst. 2006, 456, 155-162.
D. B. Varshney, X. Gao, T. Friščić, L. R. MacGillivray* "Heteroditopic Rebek's imide directs the reactivity of homoditopic olefins within desolvated quaternary assemblies in the solid-state" Angew. Chem. Int. Ed. 2006, 45, 646-650.
2005
T. Friščić, T. D. Hamilton, G. S. Papaefstathiou, L. R. MacGillivray* "A template-controlled solid-state reaction for the organic chemistry laboratory" J. Chem. Ed. 2005, 82, 1679-1681.
T. Friščić, L. R. MacGillivray* "Reversing the code of a template-directed solid-state synthesis: A bipyridine template that directs a single-crystal-to-single-crystal [2+2] photodimerization of a dicarboxylic acid" Chem. Commun. 2005, 5748-5750.
G. S. Papaefstathiou, T. Friščić, L. R. MacGillivray* "Design and construction of a 2D metal organic framework with multiple cavities: A nonregular net with a paracyclophane that codes for multiply fused nodes" J. Am. Chem. Soc. 2005, 127, 14160-14161.
L. R. MacGillivray,* G. S. Papaefstathiou, T. Friščić, D. B. Varshney, T. D. Hamilton "Template-controlled synthesis in the solid state" Topics Current Chem. 2005, 248, 201-221.
G. S. Papaefstathiou, I. G. Georgiev, T. Friščić, L. R. MacGillivray* "A photoactive one-dimensional ladder-like coordination polymer based on a dinuclear Zn(II) platform" Chem. Commun. 2005, 3974-3975.
T. N. Sokolov, T. Friščić, L. R. MacGillivray* "Crystal and molecular structure of 9,10-trans,trans-bis(4-pyridylethynyl)anthracene" J. Struc. Chem. 2005, 46, S171-S174.
T. Friščić, L. R. MacGillivray* "Single-crystal-to-single-crystal [2+2] photodimerizations: From discovery to design" Z. Krist. 2005, 220, 351-363.
T. Friščić, L. R. MacGillivray* "Cyclophanes and ladderanes: Molecular targets for supramolecular chemists" Supramol. Chem. 2005, 17, 47-51.
2004
G. S. Papaefstathiou, T. Friščić, L. R. MacGillivray* "An infinite hydrogen-bonded molecular assembly based on catechol and a bifunctional olefin" Trans. Amer. Cryst. Assoc. 2004, 39, 110-113.
T. Friščić, D. M. Drab, L. R. MacGillivray* "A test for homology: Photoactive crystalline assemblies involving linear templates based on a homologous series of phloroglucinols" Org. Lett. 2004, 6, 4647-4650.
G. S. Papaefstathiou, T. D. Hamilton, T. Friščić, L. R. MacGillivray* "Self-assembled metal-organic squares derived from linear templates as exemplified by a polydentate ligand that provides access to both a polygon and polyhedron" Chem. Commun. 2004, 270-271.
X. Gao, T. Friščić, L. R. MacGillivray* "Supramolecular construction of molecular ladders in the solid state" Angew. Chem. Int. Ed. 2004, 43, 232-236.
X. Gao, T. Friščić, G. S. Papaefstathiou, L. R. MacGillivray* "Crystal and molecular structure of Rebek's imide" J. Chem. Cryst. 2004, 34, 171-174.
2003
G. S. Papaefstathiou, T. Friščić, L. R. MacGillivray* "A regiocontrolled 'head-to-tail' [2+2] photodimerization of a stilbene involving a ternary solid based on catechol" J. Supra. Chem. 2003, 2, 227-231.
T. Friščić, L. R. MacGillivray* "Template-switching: a supramolecular strategy for the quantitative, gram-scale construction of a molecular target in the solid state" Chem. Commun., 2003, 1306-1307.
T. Friščić, L. R. MacGillivray* "Double inclusion of ferrocene within a doubly interpenetrated three-dimensional framework based on resorcin[4]arene" J. Organomet. Chem. 666, 2003, 43-48.
1998 - 2002
T. Friščić, A. J. Lough, G. Ferguson,* B. Kaitner* "Enantiomeric bis(μ-N,N'-hexamethylene-disalicylaldiminato)dicopper(II) complexes" Acta Cryst. C58, 2002, m313-m315.
Pajić, D.; Zadro,* K.; Friščić, T.; Judaš, N.; Meštrović "Magnetic relaxation in Mn12-methanoate molecular magnet" J. Magn. Magn. Mater. 242 2002, 946-948.
D. Pajić, K. Zadro,* T. Friščić, N. Judaš, E. Meštrović "Thermal relaxation and quantum tunneling of the magnetization in Mn12-acetate" Fizika A 8, 1999, 253-260.
T. Friščić, B. Kaitner,* E. Meštrović "Synthesis and structure of N,N'-butylene- and N,N'-hexylenebis(2-oxy-1-naphthaldimine)" Croat. Chem. Acta 71, 1998, 87-98.